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  Гранулирование минеральных удобрений.
Кочетков В.Н.

 
  Новые материалы
Карабасов Ю.С.

 
  Основы техники гранулирования
П.В. Классен,
И.Г. Гришаев.

 
  Гранулированный
хлористый кальций.
ГОСТ 450-77

 
  Аммофос
 
  Сушка в химической промышленности,
М.В. Лыков


Fluidized/spouting bed dryer/granulator for granular
fertilizers, calcium chloride

dryer/granulator

A dryer/granulator is a high rate vertical vessel for granular products produced from solution, pulp and melt of any moisture. It outperforms other known dryers/granulators by 5 - 7 times in terms of drying rate.

Due to process intensity the dryer/granulator processes a small amount of feedstock (1,5 - 3 tons) that results in a low process lag and a short start time (0,5 hrs) together with product residence time to conduct the process in the automatic mode.

A short time of monoammoniumphosphate dryer/granulator allows for reduced ammonia losses as well as gas consumption per ton of the end product due to the process intensity. This results in lower exhaust emissions. The high process intensity reduces the amount of construction materials used for its fabrication and investment. Its vertical arrangement saves the floor area.

The dryer/granulator is patented in Russia No.2060810, in the USA No.5316735 and in Europe No.0597092.


 

Process flow diagram

Process flow diagram

1.Dryer/granulator

2.Furnace

3.Cyclone

4.Absorber

5.Suction fan

6.Blow fan

7.Elevator

8.Screen

9.Crusher

10.Collecting bin

11.Sluice feeder

ADVANTAGES    

•    Reduction in the amount of construction materials used for dryer/granulator fabrication.

•   Reduction in specific fuel and power consumption by 20-30%.

•   Reduction in the amount of emissions to the atmosphere by 30-40-%.

•   Increase in granule strength by 1.5-2 times and decrease in dust content by several times.


SPECIFICATION

for granular ammophos as an example

 

Index

As per design
FG2,8-35NU-01

As per analog
BGS 4-22

Ammophos capacity, t/hr

20

20

Pulp moisture, %

25

25

End product moisture, %

1.5

1.5

Gas temperature, °C

 

 

inlet

300 - 1000

400 - 500

outlet

130

100

Gas velocity at inlet, m/s

40 - 50

10

Feed gas flow rate, Nm³/hr

570

710

Flue gas flow rate, Nm³/hr

36100

52200

Weight (in metal) , tons

8.3

232

Specific evaporated moisture capacity, kg/m³·hr

180

25

Specific parameters per ton of ammophos

 

 

fuel consumption, kg of arbitrary fuel

32.7

40.6

power consumption, kw·hr

31

39



The plant was awarded at international exhibitions:

In Brussel 'Eureka-97'

Gold medal

In Paris in 1988

Grand Prix

In Moscow in 2002

Silver medal

In 2004 at IY Moscow international salon of innovations & investments

Gold medal & Diploma


For granular ammophos the 10 t/h plant FG3-17NU-01 is accepted by the Interdepartmental Commission to be put into service/ In testing 1500 tons of ammophos was produced. The 20 t/h dryer/granulator FG2,8-35NU-02 was tested with pulp moisture of 30% and a positive result obtained.

The advantages of the plant for granular ammophos over fluid bed dryers/granulators, drum, spray/fluid bed and spouting dryers are as follows:

due to the heat carrier at 800-1000 °C and velocity of 40 - 50 m/s the intensity of granulation process increases by 5 - 7 times, savings in plant construction materials are several times lower, fuel and power consumption are reduced by 20 - 30% as well as exhaust emissions to the atmosphere are decreased by 30 - 40%. The granule strength as compared with the granule strength produced in drum dryers/granulators has increased by 1.5 - 2 times and dust content of the end product has decreased by several times.

The plant is competitive in case of updating, operational and new production processes.
The dryer/granulator FG2,8-35NU-03 produces granular calcium chloride at JSC Sterlitatamaksy 'Soda' to GOST 450-77 since January 2005 . The feed is 65% moisture solution. In 2006 the granular calcium chloride capacity was 4.3 t/hr with running time of 720 hrs.

Granular calcium chloride produced by the dryer/granulator FG2,8-35NU-03 features granule density and strength, lower caking and can be stored sealed bags for several months. It meets Moscow's requirements for antiacing reagents, in the winter period of 2005-2006 Moscow 20 thous.tons of granular calcium chloride of high grade to GOST 450-77 (with calcium chloride content not less than 90%). in the winter period of 2006-2007 JSC 'Soda' delivered to Moscow 22 thous.tons, in the 2007-2008 - 25 th.t., in the 2009-2010 - 25 th.t. of granular calcium chloride produced by the dryer/granulator FG2,8-35NU-03.

The author and head of development of the dryer/granulator,   Ivanov Oleg Rostislavovich, cand.sci.

Russian version


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